Reactor Pressure Control Using Back Pressure Regulators

Back pressure regulator for Catalyst Research

  • Equilibar schematic catalyst reactor

Research into new and improved catalysts is key for the advancement of products in multiple industries. For example, petrochemical companies search for improved catalysts to convert hydrocarbons into more useful and efficient energy sources. Fine chemical producers use the catalysis process to develop novel and useful organic compounds. The automotive industry continuously refines catalysts to more efficiently remove pollutants from engine exhaust.

Most catalyst research utilizes heated reactors, beginning with multiple parallel trials at the micro-scale, and gradually increasing reactor scale up to the semi-works facility that can study practical catalyst performance at the kilogram scale. Pressures vary from near 1 bar, for environmental catalysis, up to 300 bar for many petrochemical conversions.

Request a Quote Download Brochure
The Equilibar® precision back pressure regulator is designed and demonstrated to excel within the demanding requirements of catalysis research, including:

  • Ultra wide flow window, from several liters/minute down to nano flows and zero flow
  • Precision typically within 0.5% of set-point in many research applications (5X to 10X more precise than traditional spring regulators)
  • Stability during two-phase flow
  • High temperature compatibility up to 300C
  • compact design easily fits into oven, with set-point controls kept outside oven
  • PTFE/Glass diaphragms (most popular for reactor pressure control application)
  • Hastelloy C276 and SS316L bodies (typically in stock for quicker response)

 

schematic showing back pressure regulator used for two-phase catalytic reactor control

As shown above, mass flow meters are often used to control the input of various gases (and sometimes liquids) into the heated reactor containing the catalyst sample. A back pressure regulator is typically used on the exit of the reactor to maintain stable pressure control for the catalysis process. The products of reaction are monitored using gas chromatography or other forms of analysis.

 

Request a Quote Download Brochure


Application Focus: Two-Phase Flow for Research Pressure Control

Many laboratory catalysis reactors utilize a high pressure liquid separator downstream of the reactor. In addition to requiring an expensive pressure vessel, such processes typically need a liquid level control loop in parallel to the gas phase back pressure regulator. This traditional approach is complex and has several limitations.

Because the Equilibar back pressure valve provides stable pressure control in two-phase flow, it is possible to eliminate the high pressure separator and level control system downstream of the reactor.

Contact our engineers to determine which Equilibar back pressure regulator is best suited for your unique two-phase flow application.

Request a Quote Download Brochure


Equilibar EB1HP1 is an ideal catalyst research regulatorEquilibar back pressure regulators are ideal to control reactor pressure due to their high precision, wide flow range, and two-phase flow capability See  product details .

stacked high density design is ideal for catalyst researchNew stacked design allows for space savings in parallel reactor systems. Available in 1/16″ HPLC and 1/8″ autoclave tube fittings.

 

Customer Case Study - using Equilibar Back Pressure Regulator in Fischer-Tropsch Catalyst Research Application

Customer Case Study – using Equilibar Back Pressure Regulator in Fischer-Tropsch Reactor Pressure Control

 

 

Fully automated catalysis reactor system by Integrated Lab Solutions (ILS) . ILS offers many different configurations, including a 32-Parallel Fischer-Tropsch fixed bed reactor system.

 

Alternating Feeds to a Research Reactor thumb

Whitepaper: Alternating Feeds to a Research Reactor. In cooperation with Oak Ridge National Lab’s Fuels, Engines and Emissions Research Center

Work Categories

Equilibar News

Diane Jacober, team member spotlight

Team Member Spotlight: Diane Jacober, Mechanical Engineer and Marketing Specialist

We are happy to introduce Diane Jacober, a mechanical engineer who has been working as marketing specialist for Equilibar since late last year. Diane brings a unique and especially useful set of skills to Equilibar.  She earned bachelor’s and master’s degrees in engineering from Dartmouth College and has worked as a process engineer, project engineer […]

Read More